Thermo Fisher iCAP Pro X Duo Inductively Coupled Plasma Optical Emission Spectrometer (ICP-OES) – Rental Unit

Overview

The Thermo Fisher iCAP Pro X Duo is a high-performance, benchtop inductively coupled plasma optical emission spectrometer (ICP-OES) engineered for robust, interference-resistant trace elemental analysis across diverse sample matrices. Utilizing vertical torch orientation with dual-view capability—radial and axial (bidirectional) observation—the system delivers enhanced sensitivity and dynamic linear range without compromising stability or operational simplicity. The plasma source employs a solid-state, self-tuned 27.12 MHz RF generator, ensuring consistent plasma ignition and maintenance across variable sample loads and matrix compositions—including high-salt, organic, or acidic digestates. Light collection and dispersion rely on a purged echelle grating polychromator paired with a charge-injection device (CID) detector, enabling simultaneous full-spectrum acquisition from 167.021 nm to 852.145 nm at 7 pm spectral resolution. This architecture minimizes spectral overlap and supports rigorous multi-element quantification under ISO 17025, ASTM D1976, EPA Method 200.7, and USP <232>/<233> regulatory frameworks.

Key Features

• Vertical dual-view plasma torch with corrosion-resistant, quick-release semi-detachable design for rapid maintenance and reduced downtime.
• Purged echelle grating monochromator with cross-dispersing prism, thermally stabilized to ±0.1 °C for long-term wavelength reproducibility and minimal recalibration frequency.
• Three independent mass flow controllers (MFCs) for precise, real-time regulation of nebulizer gas, plasma gas, and auxiliary gas—critical for method transferability and inter-laboratory comparability.
• Integrated interlocked drain sensor system that automatically halts analysis upon detection of fluid leakage in the sample introduction path, preventing sample loss and cross-contamination.
• Three-channel peristaltic pump supporting online internal standard addition, hydride generation integration, and segmented flow configurations.
• Random-access CID detector with full-frame readout capability, enabling flexible region-of-interest (ROI) selection, background correction, and real-time spectral diagnostics.

Sample Compatibility & Compliance

The iCAP Pro X Duo accommodates aqueous digests (HNO₃, HCl, HF-based), organic solvents (with optional oxygen ashing), and diluted biological fluids. It meets essential compliance requirements for environmental testing (EPA 200.7, 6020B), clinical trace metal analysis (CLIA, CAP), pharmaceutical impurity profiling (ICH Q2(R2), USP <232>/<233>), and food safety screening (AOAC 993.14). Its hardware architecture supports audit-trail-enabled operation under FDA 21 CFR Part 11 when deployed with Qtegra ISDS software configured for GLP/GMP environments. All optical and RF subsystems are CE-marked and comply with IEC 61000-6-3 (EMC) and IEC 61010-1 (safety).

Software & Data Management

Qtegra Intelligent Scientific Data Solution (ISDS) v3.5+ provides a validated, role-based workflow platform compliant with ALCOA+ data integrity principles. Users perform method development, real-time spectral visualization, automated background correction, and multi-point calibration—all within a single interface. The software supports electronic signatures, instrument configuration logs, audit trail export (CSV/SQL), and secure user access control (admin/operator/auditor roles). Raw spectral data (.raw), processed results (.csv/.xlsx), and metadata are stored in a relational database with configurable retention policies aligned with ISO/IEC 17025 Clause 7.5.2.

Applications

• Environmental laboratories: Multi-element analysis of drinking water, wastewater, soil extracts, and airborne particulates per EPA and ISO standards.
• Pharmaceutical QC/QA: Catalyst residue testing (Pd, Pt, Ni), elemental impurities in APIs and excipients, and leachables from packaging materials.
• Geochemical and mining labs: Rapid quantification of REEs, base metals, and precious elements in rock digests and exploration samples.
• Food and agriculture: Monitoring of toxic elements (As, Cd, Pb, Hg) and nutritional minerals (Ca, Mg, Fe, Zn) in raw commodities and processed products.
• Academic and contract research: Method validation, reference material certification, and collaborative inter-laboratory studies requiring high reproducibility (RSD <1.5% for 10 ppb Mn).

FAQ

What rental terms are available for the iCAP Pro X Duo?
Short-term (1–6 months), rent-to-own (12–36 months with purchase option), and lease-to-own (36–60 months with title transfer upon final payment) models are offered.
Is preventive maintenance included in the rental agreement?
Yes—comprehensive service packages include quarterly remote diagnostics, annual on-site PM, consumables replenishment (torch, injector, nebulizer), and priority technical support.
Can the instrument be validated for GxP use during rental?
Absolutely. IQ/OQ documentation templates, URS alignment support, and qualified installation by Thermo-certified engineers are provided upon request.
Are software licenses included and transferable?
Qtegra ISDS perpetual license with maintenance subscription is bundled; license rights remain active for the duration of the rental term and may be extended or migrated upon renewal.
What happens if the instrument requires repair outside scheduled maintenance?
All rentals include 24/7 remote diagnostics and next-business-day on-site response for critical faults—covered under the service-level agreement (SLA) with no additional labor or parts fees.