Agilent Intuvo 9000–5977B GC/MS System (Refurbished)

Overview

The Agilent Intuvo 9000–5977B GC/MS System is a fully refurbished, factory-tested benchtop gas chromatography–mass spectrometry platform engineered for high-throughput, regulatory-compliant small-molecule analysis in environmental, food safety, forensic, and pharmaceutical quality control laboratories. This integrated system combines the Intuvo 9000 GC’s chip-based flow path architecture with the 5977B single quadrupole mass selective detector (MSD), delivering robust separation performance, sub-femtogram detection sensitivity, and operational reliability validated against ISO/IEC 17025 calibration protocols. The system operates on fundamental principles of gas-phase separation (partitioning across a temperature-programmed capillary column) followed by electron ionization (EI) mass spectrometric detection. Its design eliminates traditional GC pain points—including column trimming, ferrule-based leak-prone connections, and extended oven cooldown cycles—by integrating smart thermal management, inert flow path components, and real-time system diagnostics.

Key Features

• Intuvo 9000 GC: Chip-based guard column technology extends main column lifetime and prevents downstream contamination; no column cutting required.
• Smart Key-enabled flow path identification automatically loads method-appropriate parameters (e.g., column ID, dimensions, carrier gas type) into OpenLab CDS or MassHunter software.
• Direct-heated oven achieves linear, reproducible temperature ramps up to 250 °C/min (30–450 °C range), reducing cycle time by >40% versus conventional ovens.
• 5977B MSD features High-Efficiency Source (HES), increasing ion transmission efficiency by ~10× over legacy EI sources; IDL = 1.5 fg OFN (octafluoronaphthalene) at 1 pg injection.
• 7693A Autosampler supports 150-position vial capacity, dual-needle operation, and integrated sample prep (dilution, spiking, derivatization) via Easy SamplePrep software.
• MassHunter Data Acquisition & Quantitative Analysis software provides full instrument control, spectral library search (NIST, Wiley), and audit-trail-enabled reporting compliant with FDA 21 CFR Part 11.
• Energy-efficient design consumes <50% power of conventional GC systems; compatible with standard 120 V outlets without circuit upgrades.

Sample Compatibility & Compliance

The system is validated for volatile and semi-volatile organic compounds (VOCs/SVOCs) including pesticides (EPA Method 8270D), PAHs, PCBs, residual solvents (ICH Q3C), and environmental contaminants (ASTM D3699). All refurbished units undergo full functional testing per Agilent CrossLab refurbishment standards, including retention time locking verification, mass axis calibration, detector gain optimization, and leak integrity checks. Hardware and software configurations support GLP/GMP workflows: MassHunter implements electronic signatures, user role-based access control, and immutable audit trails. The inert flow path—comprising Siltek-treated transfer lines, low-bleed columns, and deactivated source components—minimizes analyte adsorption and degradation, ensuring data fidelity for thermally labile compounds.

Software & Data Management

Data acquisition, processing, and reporting are managed through Agilent MassHunter Workstation (version B.09.00 or later), which supports method development, automated calibration, batch processing, and customizable report generation. Raw data files (.D format) are stored with embedded metadata (instrument configuration, sequence logs, calibration history). For enterprise integration, OpenLab CDS can be deployed as a centralized LIMS interface with secure SQL database backend. All systems ship with licensed software, pre-installed drivers, and validated installation qualification (IQ) documentation. Remote monitoring and troubleshooting are enabled via secure HTTPS connection to the Intuvo’s embedded web server, supporting diagnostic telemetry from >100 real-time system parameters.

Applications

This GC/MS platform is routinely deployed in accredited laboratories for pesticide residue screening in fruits and vegetables (AOAC 2007.01), residual solvent quantification in APIs (USP ), hydrocarbon fingerprinting in petroleum products (ASTM D5186), and forensic toxicology screening (SWGTOX guidelines). Its high sensitivity and rapid column reconfiguration make it suitable for method transfer between R&D and QC environments. The 7693A’s sample prep automation reduces manual handling errors in multi-analyte workflows such as EPA 525.3 (drinking water contaminants), where derivatization and internal standard addition must be precisely timed and volumetrically controlled.

FAQ

Is this a factory-refurbished unit or third-party refurbished?
All instruments are refurbished by Agilent-authorized service partners under CrossLab Certified Refurbishment protocols, including full hardware inspection, firmware update, and traceable calibration using NIST-traceable standards.
What documentation accompanies the system?
Each unit ships with Certificate of Conformance, IQ/OQ test reports, MassHunter software license certificate, and a complete set of consumables (column, septa, liners, HES filaments) sufficient for 3 months of routine operation.
Can the system be upgraded to support SIM or MRM acquisition modes?
The 5977B MSD is a single quadrupole instrument and does not support MRM; however, it supports full-scan, selected ion monitoring (SIM), and auto-tune functions—all configurable within MassHunter.
Does the warranty cover both hardware and software support?
Yes—the 6-month comprehensive warranty includes onsite labor, parts replacement, remote software assistance, and one scheduled preventive maintenance visit.
Are original Agilent service contracts available post-purchase?
Eligible customers may enroll in Agilent CrossLab Care Plans (Basic, Premium, or Platinum) upon delivery, extending coverage to 1–3 years with priority response SLAs and guaranteed spare parts availability.