PIKE Infrared Spectroscopy Accessories Kit 16XX-17XX
| Brand | PIKE |
|---|---|
| Origin | USA |
| Manufacturer Type | Authorized Distributor |
| Product Origin | Imported |
| Model | 16XX-17XX |
| Price Range | USD 0–9,999 |
Overview
The PIKE Infrared Spectroscopy Accessories Kit 16XX-17XX is a modular, application-optimized collection of high-precision ATR, transmission, and reflection accessories engineered for integration with Fourier Transform Infrared (FTIR) spectrometers. Designed and manufactured in the United States, this kit enables rigorous, reproducible molecular characterization across diverse physical states—solid, liquid, and gas—under controlled thermal and environmental conditions. Its architecture supports fundamental spectroscopic measurement principles including Beer–Lambert law-based transmission, evanescent wave sampling via Attenuated Total Reflectance (ATR), and surface-sensitive specular/multi-angle diffuse reflectance. The system accommodates routine QC workflows as well as advanced research applications requiring variable temperature control, pressure compatibility, and extended optical pathlengths—making it suitable for laboratories operating under ISO/IEC 17025, ASTM E1421, or USP compliance frameworks.
Key Features
- Multi-modal sampling flexibility: seamless transition between transmission, ATR, specular reflection, and diffuse reflectance configurations without realignment
- Thermal range coverage from –80 °C to +500 °C, compatible with cryogenic dewars, Peltier stages, and high-temperature furnace cells
- Transmission accessories include fixed-path (0.1–100 mm) and variable-path cells for liquids; high-pressure (up to 200 bar) and low-temperature solid holders; gas cells with pathlengths up to 16 m and temperature-controlled jackets
- ATR modules feature fixed-angle (45° and 60°) ZnSe, Ge, or diamond crystals, plus motorized variable-angle systems supporting quantitative depth profiling of layered films and heterogeneous surfaces
- Robust mechanical design with kinematic mounting, vacuum-compatible flanges (CF-35/CF-63), and alignment-free coupling to standard FTIR beam paths (e.g., Thermo Nicolet, Bruker Tensor, PerkinElmer Frontier)
Sample Compatibility & Compliance
The 16XX-17XX kit supports organic and inorganic samples across all three phases. Solid samples include polymers, catalysts, pharmaceutical tablets, and geological specimens; liquids encompass aqueous buffers, ionic liquids, and aggressive solvents (e.g., HF, concentrated HNO₃ with chemically resistant cell windows); gases include reactive species (NH₃, Cl₂, SO₂) and isotopically labeled standards. All accessories comply with ISO 17025 calibration traceability requirements when used with certified reference materials (e.g., NIST SRM 1921b for ATR correction). Optional GMP-compliant documentation packages—including instrument qualification protocols (IQ/OQ/PQ), audit trails, and 21 CFR Part 11–ready electronic records—are available upon request.
Software & Data Management
Accessories operate natively with vendor-supplied FTIR acquisition software (OMNIC, OPUS, Spectrum) and support third-party platforms via standardized ASCII spectral export (.spa, .jdx, .csv). Real-time thermal metadata tagging (temperature, pressure, time-stamp) is embedded directly into spectral headers. For regulated environments, optional PIKE ControlSuite™ provides full audit trail logging, user role-based access control, electronic signatures, and automated report generation aligned with GLP and FDA validation expectations. All firmware updates are digitally signed and version-controlled per IEC 62443-3-3 cybersecurity guidelines.
Applications
- Pharmaceutical solid-state analysis: polymorph identification, hydrate/dehydrate kinetics, and API-excipient interaction studies under accelerated stability conditions
- Catalysis research: in situ/operando monitoring of surface adsorbates on supported metal oxides during CO oxidation or Fischer–Tropsch synthesis
- Materials science: depth-resolved compositional mapping of multilayer thin films (e.g., OLED stacks, battery SEI layers) using angle-resolved ATR
- Environmental analytics: trace gas quantification (ppb-level NOₓ, CH₄, VOCs) in ambient air or stack emissions using long-path gas cells
- Academic spectroscopy: teaching labs benefit from interchangeable modules enabling comparative method validation (e.g., KBr pellet vs. ATR vs. DRIFTS for clay mineralogy)
FAQ
Are these accessories compatible with non-PIKE FTIR spectrometers?
Yes—the 16XX-17XX series features universal beam geometry alignment and standard 25.4 mm optical mounts, ensuring interoperability with major OEM platforms.
Do ATR accessories include crystal replacement kits and cleaning protocols?
Each ATR module ships with a documented maintenance kit (crystal holder wrenches, microfiber cloths, solvent compatibility chart) and a validated cleaning SOP compliant with ISO 10418.
Can the gas cell be evacuated and backfilled with inert atmosphere?
All gas cells include dual VCR fittings, vacuum-rated seals (<1×10⁻⁶ mbar), and optional integrated mass flow controllers for dynamic gas switching.
Is technical support available for method development?
PIKE-certified application scientists provide remote and on-site method optimization services, including spectral preprocessing workflows and multivariate calibration guidance.
What documentation accompanies each shipment?
Each kit includes a Certificate of Conformance, dimensional drawings, optical performance test reports, and RoHS/REACH declarations.
